Mawardanti, Azzahra Salsabila Syifa and Maftuhah, Azizatul and Ir. Bambang Poerwadi, M.S. and Haryo Tejo Prakoso, S.Si., M.Agr.Env. (2023) Pemanfaatan Residual Oil Spent Bleaching Earth sebagai Biodiesel Menggunakan Microwave. Sarjana thesis, Universitas Brawijaya.
Abstract
Pada tahun 2022 produksi minyak sawit mentah (crude palm oil) di Indonesia mencapai 47,73 juta ton. Pada industri minyak sawit terdapat proses pemurnian minyak dengan menggunakan bleaching earth. Spent bleaching earth merupakan hasil akhir dari proses pemurnian CPO yang mengandung kadar minyak tinggi, sekitar 20-30% yang apabila dibuang ke lingkungan akan menyebabkan pencemaran tanah. Terdapat beberapa metode untuk menurunkan kadar minyak SBE salah satunya metode ekstraksi pelarut. Hasil dari ekstrasi SBE yaitu residual oil SBE yang dapat dimanfaatkan sebagai bahan baku biodiesel. Penelitian ini bertujuan untuk mengetahui perbandingan massa SBE dan pelarut, serta suhu yang optimal dalam mengekstrak residual oil SBE dan mengetahui potensi residual oil SBE dijadikan sebagai biodiesel dengan penggunnaan microwave. Ekstraski residual oil dilakukan pada variasi perbandingan massa SBE dan pelarut 1:2, 1:4, dan 1:6 pada varisi suhu 26, 40, dan 50°C. Residual oil yang telah di pretreatment dilakukan reaksi transesterifikasi dengan metanol 15% dan KOH 1% selama 10 menit pada suhu 60C menggunakan microwave. Hasil ekstraksi yang paling optimal ada pada perbandingan 1:4 pada suhu ruang dengan yield 19,12% dan percentage oil extraction (POE) 79,68%. Residual oil SBE berpotensi untuk dijadikan biodiesel dan didapatkan rendemen 33,53% dan konversi 45,28% dengan kadar FAME 92,97%.
English Abstract
Crude palm oil production in Indonesia in 2022 reached 47.73 million tons. In the palm oil industry there is an oil refining process using bleaching earth. Spent bleaching earth is the end result of the CPO refining process which contains high oil content, around 20-30%, which if disposed of into the environment will cause soil pollution. There are several methods to reduce SBE oil content, one of which is the solvent extraction method. The result of SBE extraction is SBE residual oil which can be used as raw material for biodiesel. This research aims to determine the mass ratio of SBE and solvent, as well as the optimal temperature for extracting SBE residual oil and determine the potential for SBE residual oil to be used as raw material biodiesel using a microwave. Residual oil extraction was carried out at varying mass ratios of SBE and solvent 1:2, 1:4, and 1:6 at varying temperatures of 26, 40, and 50°C. Residual oil that has been pretreated is transesterified with 15% methanol and 1% KOH for 10 minutes at 60C using a microwave. The most optimal extraction results were in a ratio of 1:4 at room temperature with a yield of 19.12% and a percentage oil extraction (POE) of 79.68%. SBE residual oil has the potential to be used as raw material biodiesel and obtained a yield of 33.53% and a conversion of 45.28% with a FAME content of 92.97%.
| Item Type: | Thesis (Sarjana) |
|---|---|
| Identification Number: | 052307 |
| Uncontrolled Keywords: | Biodiesel, Microwave, Residual Oil, Spent Bleaching Earth |
| Subjects: | 600 Technology (Applied sciences) > 665 Technology of industrial oils, fats, waxes, gases > 665.3 Vegetable fats and oils > 665.37 Biodiesel fuel |
| Divisions: | Fakultas Teknik > Teknik Kimia |
| Depositing User: | Unnamed user with username tunjungsari |
| Date Deposited: | 15 Jan 2024 08:34 |
| Last Modified: | 15 Jan 2024 08:34 |
| URI: | http://repository.ub.ac.id/id/eprint/210436 |
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